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Title: Flexible kappa(4)-PNN ' O-tetradentate ligands: synthesis, complexation and structural studies
Authors: Durran, Sean E.
Elsegood, Mark R.J.
Hammond, Shelly R.
Smith, Martin B.
Issue Date: 2010
Publisher: © Royal Society of Chemistry
Citation: DURRAN, S.E. ... et al, 2010. Flexible kappa(4)-PNN ' O-tetradentate ligands: synthesis, complexation and structural studies. Dalton Transactions, 39 (30), pp. 7136 - 7146.
Abstract: The three-step synthesis of new, air-stable, PNN′O-tetradentate ligands 3a·HH–3c·HH by Schiff base condensation of the 1° amines 2a–2c with 2-Ph2PC6H4(CHO) in refluxing EtOH is described. The racemic ligand 3d·HH, isolated in 79% yield, was successfully prepared from 2-C6H4(OH){C(O)NHCH2CH(Me)NH2} 2d and 2-Ph2PC6H4(CHO) in absolute EtOH... cont'd.
Description: This article was published in the journal Dalton Transactions [© Royal Society of Chemistry]. The definitive version is available at: http://dx.doi.org/10.1039/c0dt00200c
Sponsor: We should like to thank the EPSRC for funding, Johnson Matthey for the generous loan of precious metal salts and the EPSRC Mass Spectrometry Service Centre at Swansea. We also wish to acknowledge the use of the EPSRC’s Chemical Database Service at Daresbury.
Version: Submitted for publication
DOI: 10.1039/c0dt00200c
URI: https://dspace.lboro.ac.uk/2134/15950
Publisher Link: http://dx.doi.org/10.1039/c0dt00200c
ISSN: 1477-9226
Appears in Collections:Published Articles (Chemistry)

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