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Title: Aspects of steroidal partial synthesis and rearrangements
Authors: Silva, Rafael T.
Issue Date: 1982
Publisher: © Rafael T. Silva
Abstract: The previously reported conversion of 3ß-tosyloxy-5α-cholestane-5, 6ß-diol with Buᵗ0K/Buᵗ0H to 3ß-methyl-A-nor-5ß-cholestan-5-ol-6-one, is believed to arise from a novel intramolecular ene reaction of an intermediate unsaturated acyloin, 4,5-seco-cholest-3-en-6ß-ol-5-one. It was proposed to synthesise the unsaturated acyloin 4,5-secocholest- 3-en-6ß-ol-5-one to determine whether it would indeed undergo the ene reaction. [continues…]
Description: A Masters Thesis. Submitted in partial fulfilment of the requirements for the award of Master of Philosophy of Loughborough University.
Sponsor: National Council of Research and Technology (CONACYT), Mexico.
URI: https://dspace.lboro.ac.uk/2134/26214
Appears in Collections:MPhil Theses (Chemistry)

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